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Blogmaster: Dr. Eldridge M. Mount III

07

I recently received the following two questions by e-mail  on COF of laminates and thought you might be interested.

1.    A foil/paper laminate roll  is kept in an AC room for three months, but after three months, the non-laminated side of foil shows drop in treatment level. Can you explain the reason for such drop in treatment level of foil?

I would expect that migratory additives are transferring from the paper to the foil surface.  This would be typical.  Also there may be some oxidation of the foil changing the chemistry of the surface.  At any rate, to fully understand the changes you would have to measure the chemical changes taking place at the aluminum surface.  Specifically you would be looking for organic contamination or a change in the aluminum oxide composition or hydrolysis

2. Whether the COF (coefficient of friction) of a PET / Polyethylene laminate drops after 5 days after lamination? If the COF of laminate is 0.405 and then drops to 0.250, Is it possible and if yes then why?

Here again we have a slip migration occurring.  Typically the lamination COF is high after lamination as the surfaces are free of additive (migratory slip additives such as erucamide of Stearamide etc) due to the high melt temperatures in processing. 

As the sample cools the slip chemicals in the bulk diffuse to the film surface and create a layer of the migratory additives at the surface.  The slip materials are low molecular weight and “contaminate” the surface with a grease like coating.  This then lubricates the surface lowering the COF.

Slip migration is very sensitive to heating and cooling during processing and storage and In North America the migration is very difficult to control.  This will be true for any region where there are distinct changes in average temperatures between winter and summer.  In these variable climate regions, for many films using a migratory slip system it is necessary to have a summer and winter formulation.  In general less slip is needed in summer due to the fast migration at summer temperatures and more is needed in winter so that a sufficient amount comes to the surface.  Of course the amount needed in the winter is generally too much for the summer and the formulation slip levels have to be watched closely to prevent problems from too much surface slip (poor adhesion generally in lamination bond and or ink).

So for the migratory slip technology the two most difficult questions to be answered are; first, is it summer yet, and second, is it winter yet?

Posted in: Basics

Comments

Sunday, May 08, 2011 8:55 AM
one of our customer require a very thin laminated which is 37 PET/PE (12 micron polyester film & 25 micron PE film .due to thin film structures ,we have added 2% slip additive in sealing layer but after lamination with solvent less two component ,we got higher C.O.F above the specification limit of customer defined criteria.we have then further add some %age of high slip film grade but after lamination ,C.O.F still high from polyester to polyester side c& PE to PE Side.we have increased the time of testing & re-check the C.O.F ; C.O.F drops to some extent but not very much now we need a solution in which we get stable C.O.F after lamination and under the range of specification limit.kindly suggest that after how much time of lamiantion & slitting ,we will CHECK c.o.f,& how WE REDUCE THIS TO GET LOWER C.O.F VALUES IMEDIATLY
Sunday, May 08, 2011 8:59 AM
one of our customer require a very thin laminated which is 37 PET/PE (12 micron polyester film & 25 micron PE film .due to thin film structures ,we have added 2% slip additive in sealing layer but after lamination with solvent less two component ,we got higher C.O.F above the specification limit of customer defined criteria.we have then further add some %age of high slip film grade but after lamination ,C.O.F still high from polyester to polyester side c& PE to PE Side.we have increased the time of testing & re-check the C.O.F ; C.O.F drops to some extent but not very much now we need a solution in which we get stable C.O.F after lamination and under the range of specification limit.kindly suggest that after how much time of lamination & slitting ,we will CHECK c.o.f,& how we reduce this time and what will we do to get lower C.O.F values after lamination
Friday, August 19, 2011 9:26 AM
It was a awe-inspiring post and it has a significant meaning and thanks for sharing the information.Would love to read next post too......
Thanks
Regards
PET Preform manufacturers
Tuesday, February 07, 2012 3:32 AM
Why inks applied on corona treated polyester film pass tape adhesion test but completely transfered toward polyethylene film side after lamination with solvent less two component adhesive?Is there any test except tape test by which we can check adhesion of ink with base substrate?

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Blogmaster

Eldridge Mount photo Dr. Eldridge M. Mount III

Dr. Mount is an independent consultant in the coextrusion, extrusion, film, metallization and film converting industries. He is a leader in the development of metallized films for barrier applications and film laminations. His expertise is in oriented film product and process research, the design and implementation of extrusion systems and coextrusion die specification and system specification including installation and start-up. He is also recognized for trouble shooting mono and biaxial orientated film and sheet coextrusion, melt casting and melt pinning, and film surface treatment by corona, flame and plasma systems. EMMOUNT Technologies, LLC offers consulting and technical training in film orientation, barrier technologies, coextrusion and extrusion and measures polymer melt viscosity with a capillary rheometer.

Eldridge has over 30 years industrial experience in the extrusion and orientation of polypropylene and polyester films at ExxonMobil Chemical and ICI Americas Film Divisions. He managed the intellectual property of Mobil Chemical Films Division and has courtroom experience as an expert witness. A frequent contributor to SPE ANTEC, AIMCAL and TAPPI conferences, he is a member of the SPE Extrusion Division Board of Directors, and a Fellow and Honored Service Member of SPE. Appointed AIMCAL Metallizing Consultant in 2001 and a past VP of the Society of Plastics Engineers. He has a Bachelors degree in Chemistry from West Chester University and a ME and PhD in Chemical Engineering from Rensselear Polytechnic Institute.

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Eldridge M. Mount III

EMMOUNT Technologies, LLC

Beth M. Foederer

Optex Process Solutions, LLC